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Asian Journal of Research in Chemistry
Year : 2019, Volume : 12, Issue : 6
First page : ( 317) Last page : ( 321)
Print ISSN : 0974-4169. Online ISSN : 0974-4150.
Article DOI : 10.5958/0974-4150.2019.00058.0

Multi Component Reactions (MCR): Nano ZnO catalysed efficient synthesis of Novel Thiazolidinones

Devi Bandaru, Madhavi B., Sharma G. Veera Raghava*

Department of Chemistry, GITAM Institute of Science, GITAM (Deemed to be University), Rushikonda, Visakhapatnam, 530045, Andhra Pradesh, India

*Corresponding Author E-mail: gvrs276@gmail.com, sharmavr.ganapavarapu@gitam.edu

Online published on 19 December, 2019.

Abstract

Nano ZnO has shown to be a suitable catalyst in a multicomponent reaction involving an aldehyde, an amine, and thioglycolic acid in N,N-dimethylformamide at moderate temperature (50°C) to form thiazolidinones. This one-pot method involved reasonable reaction time, easy workup and purification procedure to furnish products in excellent yields. In particular, campholenic aldehyde obtained from α-pinene was used to synthesize medicinally useful bioactive thiazolidinones. Products were characterized by IR, 1H NMR, 2DNMR and mass spectra.

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Keywords

Nano ZnO, thiazolidinones, multi component reaction (MCR), moderate conditions, easy workup and purification.

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