(3.238.136.36)
Users online: 3955    [ij] [ij] [ij] 
Email id
 

Advances in Applied Research
Year : 2013, Volume : 5, Issue : 2
First page : ( 120) Last page : ( 123)
Print ISSN : 0974-3839.

Route sol-gel - Synthesis and characterization of nanocrystalline zirconia

Rakesh K., Sherly K.B.*

Department of Chemistry, Mar Athanasius College, Kothamangalam - 686 666, Kerala

*Corresponding author: Email: sherlykb@gmail.com

Online published on 7 April, 2014.

Abstract

Nanocrystalline zirconia was prepared by the interaction between ZrOCl2.8H2O and citric acid in sol-gel method. Reaction was carried out in aqueous phase followed by calcinations at optimum temperature. The structural and textural features were characterized by X-Ray Diffraction (XRD), Thermogravimetry/Differential Thermal Analysis (TG/DTA) and Scanning Electron Microscopy (SEM). Ammonia-Temperature Programmed Desorption (NH3-TPD) and Brunauer-Emmett-Teller (BET) surface area was used for analyzing surface features like acidity and porosity

Top

Keywords

Nanocrystalline zirconia, sol-gel.

Top

  
║ Site map ║ Privacy Policy ║ Copyright ║ Terms & Conditions ║ Page Rank Tool
557,175,834 visitor(s) since 30th May, 2005.
All rights reserved. Site designed and maintained by DIVA ENTERPRISES PVT. LTD..
Note: Please use Internet Explorer (6.0 or above). Some functionalities may not work in other browsers.