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Asian Journal of Research in Chemistry
Year : 2017, Volume : 10, Issue : 4
First page : ( 497) Last page : ( 503)
Print ISSN : 0974-4169. Online ISSN : 0974-4150.
Article DOI : 10.5958/0974-4150.2017.00081.5

Microwave assisted synthesis of chitosan epoxy asparagine hydroxamate (CE-AH) Characterization and Study of its antimicrobial activity

Singh Monika*, Loonker Sangeeta

Department of Chemistry, Jai Narain Vyas University, Jodhpur (Rajasthan),-342001, India

*Corresponding Author E-mail: mskelavat@gmail.com, sangeetag@hotmail.com

Online published on 17 October, 2017.

Abstract

Green synthetic approaches are emerged as a remarkable technology for the production of biopolymer based novel derivatives. Microwave assisted synthesis method is considered as safe alternative to conventional physiochemical methods due to its environmental friendly nature.

Chitosan was derivatized with epichlorohydrin, asparagine using microwave. After this the product was regenerated from the mixture of water and methanol (1: 1)then washed with ethanol, methanol. Solvents like DMSO, DMF are used while synthesis. The characteristics of newly formed derivative was studied by Fourier transform Infrared spectrum(FT-IR), Thermogravimetric analysis(TGA), Nuclear Magnetic Resonance(NMR), Mass spectra, Scanning Electron Microscopy(SEM), elemental analysis etc. Antimicrobial activity was studied on different bacteria and fungi by well diffusion method.

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Keywords

Microwave assisted synthesis, chitosan, asparagine, SEM, NMR, TGA antimicrobial activity.

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